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dc.contributor.authorPerevoznikov, S.S.-
dc.contributor.authorYakovlev, I.V.-
dc.contributor.authorTsybulskaya, L.S.-
dc.contributor.authorLapina, O.B.-
dc.date.accessioned2022-11-10T06:51:44Z-
dc.date.available2022-11-10T06:51:44Z-
dc.date.issued2021-
dc.identifier.citationCoatings 2021;11(9)ru
dc.identifier.urihttps://elib.bsu.by/handle/123456789/288726-
dc.description.abstractNickel phosphides NixPy are a promising family of binary compounds that have shown much promise in various fields of technology, including energy storage, light absorption and heterogeneous catalysis in the reactions of biomass hydrogenation. The performance of NixPy-containing materials depends greatly on their morphology and phase composition and, in turn, on the synthesis technique. In this work, we have employed the electroplating approach to synthesize a Ni-P coating, which was treated with nitric acid in order to develop its surface area and enrich it with phosphorus. We have employed scanning electron microscopy, X-ray diffraction and31P nuclear magnetic resonance techniques to characterize the particles separated from the coating with ultrasound for the convenience of the study. According to experimental data, the obtained powder contained a mixture of Ni3P and phosphorus oxides, which transformed into nickel phosphide phases richer with phosphorus, such as Ni5P2 and Ni12P5, after treatment at elevated temperatures. Thus, we have demonstrated that electroplating followed by acid treatment is a feasible approach for the synthesis of Ni-P coatings with increased surface area and variable phase composition.ru
dc.description.sponsorshipFunding: The reported study was funded by RFBR and BRFBR according to the research project No. 19-53-04017. I.V.Y. and O.B.L. acknowledge that this work was partially supported by the Ministry of Science and Higher Education of the Russian Federation within the governmental order for Boreskov Institute of Catalysis (project AAAA-A21-121011390054-1).ru
dc.language.isoenru
dc.publisherMDPIru
dc.rightsinfo:eu-repo/semantics/openAccessru
dc.subjectЭБ БГУ::ЕСТЕСТВЕННЫЕ И ТОЧНЫЕ НАУКИ::Химияru
dc.subjectЭБ БГУ::ТЕХНИЧЕСКИЕ И ПРИКЛАДНЫЕ НАУКИ. ОТРАСЛИ ЭКОНОМИКИ::Электроника. Радиотехникаru
dc.subjectЭБ БГУ::ТЕХНИЧЕСКИЕ И ПРИКЛАДНЫЕ НАУКИ. ОТРАСЛИ ЭКОНОМИКИ::Машиностроениеru
dc.titleSynthesis and composition study of electrochemically deposited Ni-P coating with increased surface arearu
dc.typearticleru
dc.rights.licenseCC BY 4.0ru
dc.identifier.DOI10.3390/coatings11091071-
dc.identifier.scopus85114728835-
Располагается в коллекциях:Статьи сотрудников НИИ ФХП

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